Over the next few months we will be populating this page with downloads of our pulse sequences, data, hints and tips.
EXACT ASAP HSQC
By using burst-sampling (EXACT) acquisition, this method allows the rapid acquisition of HSQC spectra, with essentially no relaxation delay (originally reported by Luy et al), but with reduced power demands making this perfectly safe on all spectrometers. Combined with non-uniform sampling in F1 it is possible to acquire 2D datasets in just a few seconds.
Sequence: The sequence and associated Bruker files including sample spectra of a fully F1-sampled and 50% NUS sampled EXACT ASAP-HSQC data can be downloaded from here
Paper: The research paper is available here.
EXACT PSYCHE and ZANGGER-STERK PURESHIFT
By using burst-sampling (EXACT) acquisition, these methods allow the pseudo-2D (interferrogram) acquistion of PSYCHE and Zangger-Sterk Pureshift data in <50% of the experiment time of the original methods.
The sequences (Bruker format) can be downloaded from here
The research paper is available here